China Dairy ›› 2026, Vol. 0 ›› Issue (3): 80-87.doi: 10.12377/1671-4393.26.03.12

• QUALITY CONTROL • Previous Articles     Next Articles

Optimization and Comparative Study of Iodine Content Detection Method in Milk Based on Gas Chromatograph

HUANG Yawei, HOU Xiaofeng, CAO Wenyan*, WANG Meina, ZHANG Xiao, MA Jianjun, ZHAI Jing   

  1. Baoding Mengniu Beverage Co.,Ltd.,Hebei Province Key Laboratory of Intelligent Testing Technology for Dairy Products,Baoding Hebei 072450
  • Online:2026-03-25 Published:2026-04-09

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Abstract: [Objective] This study focused on the optimization of the sample pretreatment process for the determination of iodine content in food by gas chromatography stipulated in“GB 5009.267—2020 Food Safety National Standard Determination of Iodine in Food”,aiming to reduce the detection cost,shorten the detection time,and improve the detection efficiency and accuracy. [Method] Replace the separatory funnel with a centrifuge tube to reduce the sample weighing,increase the number of vortexing and centrifugation,and optimize the amount of butanone added to explore the optimal detection method. [Result] The optimized gas chromatography method demonstrated excellent performance in terms of recovery rate,precision,repeatability and detection limit when compared with the gas chromatography method specified in the national standard. [Conclusion] By overcoming the cumbersome problem of pretreatment,the optimized gas chromatography method was possible to accurately and quickly determine the iodine content in milk,and it was suitable for the large-scale detection of iodine content in milk.

Key words: iodine, milk, Gas Chromatography（GC）

[1] 谭进衍,气相色谱法测定奶粉中碘的含量前处理方法改良[J].中国食品,2018(18):131-133.
[2] 吴伯龙. 吉林省碘缺乏病防治现状及策略研究[D].长春:吉林大学,2014.
[3] 于园,冯波.碘与甲状腺疾病的研究进展[J].药品评价,2015(9):45-48.
[4] 中国营养学会.中国居民膳食营养素参考摄入量(2023版)[M].北京:科学出版社,2023.
[5] 何海茵,李南,余春丽,等.气相色谱法测定食盐中的碘含量[J].食品安全质量检测学报,2020,11(16):5494-5500.
[6] 王树奇. 气相色谱法测定乳粉中碘含量样品前处理方案的探讨和优化[J].现代食品,2022,28(13):156-160.
[7] 朱洁,李卓,周优.气相色谱法测定乳制品中碘含量的分析与优化[J].现代食品,2018(23):79-82.
[8] 梁琳. 气相色谱法测定液态乳中碘含量的方法优化[J].乳业科学与技术,2025,48(2):15-19.
[9] 黄会秋. 气相色谱法测定加碘食盐中碘[J].食品科学,2002,23(1):122-123.
[10] 国家卫生和计划生育委员会,国家食品药品监督管理总局.GB5009.267—2020食品安全国家标准食品中碘的测定[S].
[11] 中华人民共和国国家质量监督检验检疫总局,中国国家标准化管理委员会.GB/T 27404—2008 实验室质量控制规范食品理化检测[S].
[12] 中华人民共和国国家卫生健康委员会,国家市场监督管理总局.GB/T5009.295—2023 食品安全国家标准化学分析方法验证通则[S].
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