China Dairy ›› 2022, Vol. 0 ›› Issue (7): 65-69.doi: 10.12377/1671-4393.22.07.14

• QUALITY CONTROL • Previous Articles     Next Articles

Study on the Stability of Vitamin D3 InInfant Formula Milk Powder under Different Storage Conditions

WANG Fang1, BAO Yihong1, LAN Huijuan1   

  1. 1Quality Inspection Center of BeiDaHuang Wandersun Dairy Holdings Co.,Ltd.,Harbin Heilongjiang150078;
    2College of Forestry,Northeast Forestry University,Harbin Heilongjiang 150078
  • Online:2022-07-25 Published:2022-08-02

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Abstract: The stability of fat-soluble vitamin D3 in infant formula milk powder（referred to as "infant formula"） during storage was tracked and studied. Test method：after saponifying,extracting,purifying and concentrating 3 kinds of infant formula powders with potassium hydroxide ethanol solution,they were prepared by normal-phase high-performance liquid chromatography column,separated by reverse-phase C18 high-performance liquid chromatography column,and detected by ultraviolet detector and external standard quantitative method. Test results：when the weighing sample of infant formula powder is 10.0 g and the constant volume is 2 mL,the detection limit of the method is 0.303 μg/100g,and the quantification limit of the method is 0.909 μg/100 g. In this range,the linear regression equation Y=3.3608X+0.0388,at this time R2=0.999 1. Conclusion：the content of vitamin D3 in infant formula is less affected by normal temperature and cool and dry environment,the content of fat-soluble vitamin D3 decreases due to temperature decomposition under low and high temperature conditions with prolonged storage time.

Key words: infant formula, Vitamin D3, stability, storage conditions

CLC Number: 

  • TS252.51
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