中国乳业 ›› 2024, Vol. 0 ›› Issue (5): 94-97.doi: 10.12377/1671-4393.24.05.18

• 质量安全 • 上一篇    下一篇

乳品生产过程中折光仪法检测过氧化氢的研究

鲍晓凤, 赵晶晶*, 张春丽, 顾春光, 杨留岱, 张广福, 陈娟   

  1. 内蒙古蒙牛乳业科尔沁有限责任公司检测实验室,内蒙古通辽 028000
  • 出版日期:2024-05-25 发布日期:2024-06-11
  • 通讯作者: *赵晶晶(1990-),女,内蒙古通辽人,本科,研究方向为食品分析检验。
  • 作者简介:鲍晓凤(1981-),女,辽宁沈阳人,硕士,质量工程师,研究方向为食品分析检验;张春丽(1991-),女,内蒙古通辽人,本科,研究方向为食品分析检验;顾春光(1983-),女,内蒙古通辽人,本科,质量工程师,研究方向为食品分析检验;杨留岱(1975-),男,内蒙古通辽人,本科,研究方向为食品分析检验;张广福(1980-),男,内蒙古呼和浩特人,本科,研究方向企业管理;陈 娟(1987-),女,内蒙古呼和浩特人,本科,质量工程师,研究方向食品安全。

Research on the Detection of Hydrogen Peroxide by Refractometer Method in Dairy Production Process

BAO Xiaofeng, ZHAO Jingjing*, ZHANG Chunli, GU Chunguang, YANG Liudai, ZHANG Guangfu, CHEN Juan   

  1. Testing Laboratory,Inner Mongolia Mengniu Dairy Horqin Co.,Ltd.,Tongliao Inner Mongolia 028000
  • Online:2024-05-25 Published:2024-06-11

摘要: [目的]以过氧化氢为对象,收集0%~50%含量过氧化氢用于测试,研究含量、温度、时间3 个因素对折光法检测结果的影响,指导日常检测。[方法]鉴于不同浓度的同类物质对光的折射率不同,且浓度变化与折射率变化在一定范围内成反比例关系,双氧水折光仪利用这一特性,通过检测样品折射角差异可自动计算待测样品浓度。[结果](1)对同一试样用折光仪法测试,结果离散性小、数据稳定,与国标方法相关性好。(2)不同含量过氧化氢分别用折光仪法和国标方法检测,结果偏差最大0.3%、最小0.0%,样品含量高低对结果准确性无影响。(3)折光仪检测温度需≤35 ℃,保证样品温度为20~35 ℃,用折光仪检测能获得准确数值。(4)测试时间超过50 s,检测值会发生变动,建议日常检测控制在50 s内读数。[结论]用折光仪法检测过氧化氢浓度快速准确,操作简单便捷。需注意样品温度和检测时间在操作过程中的影响。

关键词: 折光仪, 过氧化氢, 高准确度, 易于操作

Abstract: [Objective] Hydrogen peroxide is used as a packaging disinfectant in dairy production, and its content needs to be tested before and after heating. This study focused on hydrogen peroxide and collected hydrogen peroxide with a content of 0% to 50% for testing. The study investigated the effects of three factors, namely content, temperature, and time, on the results of refractive index detection, providing guidance for daily testing. [Method] In view of the different concentrations of similar substances have different refractive indices of light,and the concentration change is inversely proportional to the refractive index change within a certain range,the hydrogen peroxide refractometer can automatically calculate the concentration of the samples by detecting the difference in the refraction angle of the samples. [Result] (1)The same sample was tested by refractometer method,the results were less discrete,the data was stable,and the correlation with the national standard method was good.(2)Different cotents of hydrogen peroxide were detected by refractometer method and national standard method respectively,the deviation of results was 0.3% and 0.0% respectively,and the sample content had no influence on the accuracy of the results.(3)The detection temperature of refractometer should be ≤35 ℃ to ensure that the sample temperature is 20~35 ℃,and the accurate value can be obtained by the detection of the refractometer.(4)If the test time exceeded 50 s,the detection value would change.It is recommended to control the reading within 50 s for daily testing. [Conclusion] Using refractometer method to detect hydrogen peroxide concentration is a fast,accurate and easy to operate.It is necessary to pay attention to the influence of sample temperature and detection time during operation.

Key words: refractometer, hydrogen peroxide, high accuracy, easy to operate

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