羧甲基纤维素钠对风味发酵乳中脂肪测定的影响

doi:10.12377/1671-4393.22.06.17

摘要/Abstract

摘要： 通过对风味发酵乳添加不同含量水平的羧甲基纤维素钠（CMC-Na）、不同种类的增稠剂以及采集含有不同增稠剂的市售风味发酵乳,采用《GB 5009.6—2016食品安全国家标准食品中脂肪的测定》中第三法碱水解法对各样品中脂肪进行测定,深入分析CMC-Na对风味发酵乳中脂肪测定的影响。结果表明：CMC-Na的添加量为0.10%和0.25%时对脂肪检测结果基本无影响,但从0.50%的添加量开始,随着CMC-Na的添加量水平越高,脂肪测定结果越低;针对目前应用较多的9 种增稠剂,统一选取1%的添加量水平,与CMC-Na进行种类间对比,其中果胶、羟丙基二淀粉磷酸酯、琼脂、乙酰化淀粉二磷酸酯、明胶、卡拉胶、海藻酸钠共7 种增稠剂对风味发酵乳中脂肪测定结果基本无影响,但结冷胶和黄原胶与CMC-Na情况类似,会使得风味发酵乳中脂肪检测结果偏低;针对20 款市售风味发酵乳进行脂肪测定,其中含CMC-Na的两款产品脂肪检测结果与标示值相差较大,且低于产品标准要求,其余未加CMC-Na的风味发酵乳的脂肪测定结果则与标示值接近。这为风味发酵乳中脂肪测定结果的准确判定以及产品的多样化发展提供一定参考。

关键词: 羧甲基纤维素钠（CMC-Na）, 风味发酵乳, 脂肪

Abstract: By adding different levels of sodium carboxymethyl cellulose（CMC-Na）and different thickeners to flavor fermented milk and collecting commercial flavor fermented milk with different thickeners,the fat in each sample was determined by the third method（alkali hydrolysis method）of GB 5009.6—2016. The effect of CMC-Na on the determination of fat in flavor fermented milk was deeply analyzed. The results showed that the addition of 0.10 % and 0.25 % CMC-Na had no effect on the fat determination results,but from the addition of 0.50%,the higher the addition level of CMC-Na,the lower the fat determination results. At the level of 1%,9 thickeners which are widely used in the market were compared with CMC-Na. Among them,pectin,hydroxypropyl starch phosphate,agar,acetylated starch diphosphate,gelatin,carrageenan and sodium alginate had no effect on the determination of fat in fermented milk,but gellan gum and xanthan gum were similar to CMC-Na. It will make the fat detection results lower in the fermented milk. The fat of 20 commercial flavor fermented milk was determined. The fat test results of two products containing CMC-Na were quite different from the marked value and lower than the product standard requirements. The fat test results of other flavor fermented milk without CMC-Na were close to the label value. This provides a certain reference for the accurate determination of fat in flavor fermented milk and the diversified development of products.

Key words: sodium carboxymethyl cellulose （CMC-Na）, flavor fermented milk, fat

中图分类号:

TS252.54

刘芳芳, 彭程程, 吴倩, 薛敏敏, 邓凌云. 羧甲基纤维素钠对风味发酵乳中脂肪测定的影响[J]. 中国乳业, 2022, 0(6): 87-93.

LIU Fangfang, PENG Chengcheng, WU Qian, XUE Minmin, DENG Lingyun. Effect of Sodium Carboxymethyl Cellulose on Determination of Fat in Flavor Fermented Milk[J]. China Dairy, 2022, 0(6): 87-93.

参考文献

[1] 中华人民共和国卫生部. GB 19302—2010食品安全国家标准发酵乳[S]. 北京: 中国标准出版社, 2010.
[2] Ishida H.Milk,daily products and bone health nutritional value of milk and dairy products[J]. Clinical Calcium,2018,28(4):483-491.
[3] Baars T,Berge A C,Garssen J, et al.Effect of raw milk consumption on perceived health, mood and immune functioning among US adults with a poor and normal health:a retrospective questionnaire based study[J]. Complementary Therapies in Medicine,2019,47:102196.
[4] Ashraf R,Shah N P.Selective and differential enumerations of Lactobacillus delbrueckii subsp. bulgaricus,Streptococcus thermophilus,Lactobacillus acidophilus,Lactobacillus casei and Bifidobacterium spp. in yoghurt: a review[J]. International Journalof Food Microbiology,2011,149:194-208.
[5] 王丹,丹彤,孙天松,等. SPME-GC-MS结合ROAV分析单菌及复配发酵牛乳中关键性风味物质[J]. 食品科学,2017,38(8):145-152.
[6] Ngongang E F T,Tiencheu B,Achidi A U,et al. Effects of probiotic bacteria from yogurt on enzyme and serum cholesterol levels of experimentally induced hyperlipidemic Wistar albino rats[J]. American Journal of Biology and Life Sciences,2016,4:48-55.
[7] 李蕊,王一然,刘一鸣, 等. 不同益生元对酸奶游离氨基酸及风味的影响[J]. 食品科学,2020, 41(20):83-89.
[8] Mcfarland L V.From yaks to yogurt:the history,development,and current use of probiotics[J]. Clinical Infectious Diseases,2015,60(Suppl 2):85-90.
[9] 任雪明,姚晶,张俊山,等.干酪风味褐色发酵乳的加工工艺及风味物质研究[J].食品安全质量检测学报,2021,12(15):6213-6221.
[10] 周禹池,吴起,熊玲,等. 魔芋葡甘聚糖羧甲基化食品增稠剂的制备及分析[J].食品科学,2014, 35(22):1-5.
[11] 如意,任冬艳,刘文俊,等. 塔什干地区发酵乳制品中酵母菌的分离鉴定[J].中国乳品工业, 2021, 49(7):13-17.
[12] 李昊泽,石丽丽,曹学丽,等. 风味发酵乳中香精关注成分的筛选及暴露风险评估[J].食品科学, 2021,42(18):254-260.
[13] 吴丽萍,孙虹,董康珍. 改性燕麦麸水溶性膳食纤维对发酵乳品质及抗氧化活性的影响[J].食品与生物技术学报,2021, 40(9): 40-49.
[14] 任静波, 任丽哲.食品添加剂在发酵乳制品中的应用[J].中国乳业, 2021,(4):85-88.
[15] 孙亚婷. 发酵乳饮料的调配与聚合乳清蛋白对发酵乳饮料稳定性的影响:[硕士论文][D]. 哈尔滨:东北农业大学,2016.
[16] 胡国华. 功能性食品胶[M]. 北京:化学工业出版社, 2014.
[17] 陈一萌, 李思宁,唐善虎,等. 不同稳定剂对凝固型牦牛酸奶在冷藏后熟过程中品质及风味的影响[J].食品工业科技,2018,39(4):188-196.
[18] Fuquay J W,Herr B.Additives in dairy foods:types and functions of additives in dairy products encyclopedia of dairy sciences (second edition)[M]. San Diego: Academic Press,2011.
[19] Burgardt V C F,Zuge L C B,Bonna S G,et al. The addition of carboxymethyl cellulose in caseinomacropeptide acid gels:rheological,optical and microstructural characteristics[J].Food Hydrocolloids, 2015,11(2):1-11.
[20] 刁静静. 羧甲基纤维素钠[J].肉类研究, 2010(3): 66-68.
[21] Du B,Li J,Zhang H, et al.The stabilization mechanism of acidified milk drinks induced by carboxymethyl cellulose[J]. Le Lait,2007,87:287-300.
[22] 李静. 羧甲基纤维素钠溶液的流变性质及其对酸性乳体系的稳定作用:[硕士论文][D].上海:上海交通大学,2007.
[23] 陈躬瑞,郑玉锖,陈儒明,等. 添加羧甲基纤维素稳定酸性乳饮料胶体体系[J].福州大学学报(自然科学版),1996,1(24) 115-120.
[24] 宋艳梅,刘玉英,夏忠悦,等. 酸奶中脂肪含量检测差异影响因素的研究[J].食品安全质量检测学报,2021,12(6):2146-2152.
[25] 邱蓉. CMC和大豆多糖对酸性乳饮料中酪蛋白稳定机理的研究:[硕士论文][D]. 杭州: 浙江工商大学, 2010.
[26] Du B Q,Li J,Zhang H B,et al.Influence of molecular weight and degree of substitution of Carboxymethyl cellulose on the stability of acidified milk drinks[J]. Food Hydrocolloids,2009,23(5): 1420-1426.
[27] 晏凯,刘晓彤,刘悦,等. 碱水解法测定乳及乳制品中脂肪的含量[J]. 食品安全质量检测学报, 2020,11(1):82-85.
[28] 吴晓静. 碱水解法测定乳粉中脂肪含量[J].食品安全导刊,2018(5):63-64.
[29] 刘祥. 高粘度羧甲基纤维素钠的研制[J].安徽工业大学学报, 2001(2):114-116.
[30] 张丽平,余晓琴. 羧甲基纤维素钠(CMC)在食品工业应用的情况和研究动态[J]. 2006, 1:119-125.
[31] 赵红玲,李全阳,陈文贞.羧甲基纤维素钠对搅拌型酸奶结构特性影响的初步研究[J]. 乳业科学与技术,2009,32(6): 282-298.
[32] 杨金姝. 羧甲基纤维素钠在食品工业中的应用研究[J]. 农产品加工,2014(11):76-78.

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